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Modern Analytical Chemistry - Online Course

Modern Analytical Chemistry - Medical Course Subject



Modern Analytical Chemistry




Introduction


1. Modern Analytical Chemistry: Introduction
2. What Is Analytical Chemistry?
3. The Analytical Perspective
4. Common Analytical Problems



Basic Tools of Analytical Chemistry


1. Numbers in Analytical Chemistry
2. Units for Expressing Concentration
3. Stoichiometric Calculations
4. Basic Equipment and Instrumentation of Analytical Chemistry
5. Preparing Solutions of Analytical Chemistry
6. Analytical Chemistry: The Laboratory Notebook



The Language of Analytical Chemistry


1. Language of Analytical Chemistry
2. Language of Analytical Chemistry: Analysis, Determination, and Measurement
3. Language of Analytical Chemistry: Techniques, Methods, Procedures, and Protocols
4. Classifying Analytical Techniques
5. Selecting an Analytical Method
6. Language of Analytical Chemistry: Developing the Procedure
7. Language of Analytical Chemistry: Protocols
8. The Importance of Analytical Methodology



Evaluating Analytical Data


1. Evaluating Analytical Data
2. Characterizing Measurements and Results
3. Analytical Data: Characterizing Experimental Errors
4. Propagation of Uncertainty
5. The Distribution of Measurements and Results
6. Statistical Analysis of Data
7. Statistical Methods for Normal Distributions
8. Detection Limits



Calibrations Standardizations and Blank Corrections


1. Calibrations, Standardizations, and Blank Corrections
2. Calibrating Signals
3. Standardizing Methods
4. Reagents Used as Standards
5. Standardizing Methods: Single-Point versus Multiple-Point Standardizations
6. Standardizing Methods: External Standards
7. Standardizing Methods: Standard Additions
8. Standardizing Methods: Internal Standards
9. Linear Regression and Calibration Curves
10. Blank Corrections



Equilibrium Chemistry


1. Equilibrium Chemistry
2. Reversible Reactions and Chemical Equilibria
3. Thermodynamics and Equilibrium Chemistry
4. Manipulating Equilibrium Constants
5. Equilibrium Constants for Chemical Reactions
6. Equilibrium Constants for Precipitation Reactions
7. Equilibrium Constants for Acid�Base Reactions
8. Equilibrium Constants for Complexation Reactions
9. Equilibrium Constants for Oxidation�Reduction Reactions
10. Le Chatelier�s Principle
11. Ladder Diagrams
12. Ladder Diagrams for Acid�Base Equilibria
13. Ladder Diagrams for Complexation Equilibria
14. Ladder Diagram for Oxidation�Reduction Equilibria
15. Solving Equilibrium Problems
16. A Simple Problem: Solubility of Pb(IO3)2 in Water
17. A More Complex Problem: The Common Ion Effect
18. Systematic Approach to Solving Equilibrium Problems
19. Solving Equilibrium Problems: pH of a Monoprotic Weak Acid
20. Solving Equilibrium Problems: pH of a Polyprotic Acid or Base
21. Effect of Complexation on Solubility
22. Buffer Solutions
23. Activity Effects
24. Two Final Thoughts About Equilibrium Chemistry



Obtaining and Preparing Samples for Analysis


1. Obtaining and Preparing Samples for Analysis
2. The Importance of Sampling
3. Designing A Sampling Plan
4. Where to Sample the Target Population
5. What Type of Sample to Collect
6. How Much Sample to Collect
7. How Many Samples to Collect
8. Minimizing the Overall Variance
9. Implementing the Sampling Plan
10. Implementing the Sampling Plan: Solutions
11. Implementing the Sampling Plan: Gases
12. Implementing the Sampling Plan: Solids
13. Separating the Analyte from Interferents
14. General Theory of Separation Efficiency
15. Classifying Separation Techniques
16. Classifying Separation Techniques: Separations Based on Size
17. Classifying Separation Techniques: Separations Based on Mass or Density
18. Classifying Separation Techniques: Separations Based on Complexation Reactions (Masking)
19. Classifying Separation Techniques: Separations Based on a Change of State
20. Classifying Separation Techniques: Separations Based on a Partitioning Between Phases
21. Liquid�Liquid Extractions
22. Separation Versus Preconcentration



Gravimetric Methods of Analysis


1. Overview of Gravimetry
2. Precipitation Gravimetry
3. Theory and Practice of Precipitation Gravimetry: Solubility Considerations
4. Theory and Practice of Precipitation Gravimetry: Avoiding Impurities
5. Theory and Practice of Precipitation Gravimetry: Occlusions
6. Theory and Practice of Precipitation Gravimetry: Controlling Particle Size
7. Theory and Practice of Precipitation Gravimetry: Filtering the Precipitate
8. Theory and Practice of Precipitation Gravimetry: Rinsing the Precipitate
9. Theory and Practice of Precipitation Gravimetry: Drying the Precipitate
10. Theory and Practice of Precipitation Gravimetry: Composition of Final Precipitate
11. Theory and Practice of Precipitation Gravimetry: Representative Method
12. Precipitation Gravimetry: Quantitative Applications
13. Precipitation Gravimetry: Qualitative Applications
14. Precipitation Gravimetry: Evaluating Precipitation Gravimetry
15. Volatilization Gravimetry
16. Volatilization Gravimetry: Theory and Practice
17. Volatilization Gravimetry: Quantitative Applications
18. Evaluating Volatilization Gravimetry
19. Particulate Gravimetry
20. Particulate Gravimetry: Theory and Practice
21. Particulate Gravimetry: Quantitative Applications
22. Particulate Gravimetry: Evaluating Particulate Gravimetry



Titrimetric Methods of Analysis


1. Titrimetric Methods of Analysis
2. Overview of Titrimetry
3. Titrations Based on Acid�Base Reactions
4. Acid�Base Titration Curves
5. Selecting and Evaluating the End Point - Titrations Based on Acid�Base Reactions
6. Titrations in Nonaqueous Solvents
7. Titrations Based on Acid�Base Reactions: Representative Method
8. Titrations Based on Acid�Base Reactions: Quantitative Applications
9. Titrations Based on Acid�Base Reactions: Qualitative Applications
10. Titrations Based on Acid�Base Reactions: Characterization Applications
11. Evaluation of Acid�Base Titrimetry
12. Titrations Based on Complexation Reactions
13. Chemistry and Properties of EDTA
14. Complexometric EDTA Titration Curves
15. Selecting and Evaluating the End Point - Titrations Based on Complexation Reactions
16. Representative Method - Titrations Based on Complexation Reactions
17. Quantitative Applications - Titrations Based on Complexation Reactions
18. Evaluation of Complexation Titrimetry
19. Titrations Based on Redox Reactions
20. Redox Titration Curves
21. Selecting and Evaluating the End Point - Titrations Based on Redox Reactions
22. Representative Method - Titrations Based on Redox Reactions
23. Quantitative Applications - Titrations Based on Redox Reactions
24. Evaluation of Redox Titrimetry
25. Precipitation Titrations
26. Precipitation Titration Curves
27. Selecting and Evaluating the End Point - Precipitation Titrations
28. Quantitative Applications - Precipitation Titration
29. Evaluation of Precipitation Titrimetry - Precipitation Titration



Spectroscopic Methods of Analysis


1. Spectroscopic Methods of Analysis
2. Overview of Spectroscopy
3. Basic Components of Spectroscopic Instrumentation
4. Spectroscopy Based on Absorption
5. Absorbance of Electromagnetic Radiation - Spectroscopy Based on Absorption
6. Transmittance and Absorbance - Spectroscopy Based on Absorption
7. Absorbance and Concentration: Beer�s Law
8. Limitations to Beer�s Law
9. Ultraviolet-Visible and Infrared Spectrophotometry
10. Instrument Designs for Molecular UV/Vis Absorption - Ultraviolet-Visible and Infrared Spectrophotometry
11. Instrument Designs for Infrared Absorption - Ultraviolet-Visible and Infrared Spectrophotometry
12. Quantitative Applications - Ultraviolet-Visible and Infrared Spectrophotometry
13. Qualitative Applications - Ultraviolet-Visible and Infrared Spectrophotometry
14. Characterization Applications - Ultraviolet-Visible and Infrared Spectrophotometry
15. Evaluation - Ultraviolet-Visible and Infrared Spectrophotometry
16. Atomic Absorption Spectroscopy
17. Instrumentation - Atomic Absorption Spectroscopy
18. Quantitative Applications - Atomic Absorption Spectroscopy
19. Evaluation - Atomic Absorption Spectroscopy
20. Spectroscopy Based on Emission
21. Molecular Photoluminescence Spectroscopy
22. Molecular Fluorescence and Phosphorescence Spectra - Molecular Photoluminescence Spectroscopy
23. Instrumentation - Molecular Photoluminescence Spectroscopy
24. Quantitative Applications Using Molecular Luminescence
25. Evaluation - Molecular Photoluminescence Spectroscopy
26. Atomic Emission Spectroscopy
27. Atomic Emission Spectra - Atomic Emission Spectroscopy
28. Equipment - Atomic Emission Spectroscopy
29. Quantitative Applications - Atomic Emission Spectroscopy
30. Evaluation - Atomic Emission Spectroscopy
31. Spectroscopy Based on Scattering



Electrochemical Methods of Analysis


1. Classification of Electrochemical Methods
2. Potentiometric Methods of Analysis
3. Potentiometric Measurements - Potentiometric Methods of Analysis
4. Reference Electrodes - Potentiometric Methods of Analysis
5. Metallic Indicator Electrodes - Potentiometric Methods of Analysis
6. Membrane Electrodes - Potentiometric Methods of Analysis
7. Membrane Potentials - Potentiometric Methods of Analysis
8. Selectivity of Membranes - Potentiometric Methods of Analysis
9. Glass Ion-Selective Electrodes - Potentiometric Methods of Analysis
10. Crystalline Solid-State Ion-Selective Electrodes - Potentiometric Methods of Analysis
11. Liquid-Based Ion-Selective Electrodes - Potentiometric Methods of Analysis
12. Gas-Sensing Electrodes - Potentiometric Methods of Analysis
13. Potentiometric Biosensors - Potentiometric Methods of Analysis
14. Quantitative Applications - Potentiometric Methods of Analysis
15. Evaluation - Potentiometric Methods of Analysis
16. Coulometric Methods of Analysis
17. Controlled-Potential Coulometry
18. Controlled-Current Coulometry
19. Quantitative Applications - Coulometric Methods of Analysis
20. Characterization Applications - Coulometric Methods of Analysis
21. Evaluation - Coulometric Methods of Analysis
22. Voltammetric Methods of Analysis
23. Voltammetric Measurements
24. Current in Voltammetry
25. Shape of Voltammograms
26. Quantitative and Qualitative Aspects of Voltammetry
27. Voltammetric Techniques
28. Quantitative Applications - Voltammetric Methods of Analysis
29. Characterization Applications - Voltammetric Methods of Analysis
30. Evaluation - Voltammetric Methods of Analysis



Chromatographic and Electrophoretic Methods


1. Overview of Analytical Separations
2. General Theory of Column Chromatography
3. Chromatographic Resolution - Theory of Column Chromatography
4. Capacity Factor - Theory of Column Chromatography
5. Column Selectivity - Theory of Column Chromatography
6. Column Efficiency - Theory of Column Chromatography
7. Peak Capacity - Theory of Column Chromatography
8. Nonideal Behavior - Theory of Column Chromatography
9. Optimizing Chromatographic Separations
10. Optimizing Chromatographic Separations Using the Capacity Factor to Optimize Resolution
11. Optimizing Chromatographic Separations Using Column Selectivity to Optimize Resolution
12. Optimizing Chromatographic Separations Using Column Efficiency to Optimize Resolution
13. Gas Chromatography: Mobile Phase
14. Gas Chromatography: Chromatographic Columns
15. Gas Chromatography: Stationary Phases
16. Gas Chromatography: Sample Introduction
17. Gas Chromatography: Temperature Control
18. Gas Chromatography: Detectors for Gas Chromatography
19. Gas Chromatography: Quantitative Applications
20. Gas Chromatography: Qualitative Applications
21. Gas Chromatography: Representative Method
22. Gas Chromatography: Evaluation
23. High-Performance Liquid Chromatography (HPLC)
24. High-Performance Liquid Chromatography Columns
25. High-Performance Liquid Chromatography (HPLC): Stationary Phases
26. High-Performance Liquid Chromatography (HPLC): Mobile Phases
27. High-Performance Liquid Chromatography Plumbing
28. High-Performance Liquid Chromatography (HPLC): Sample Introduction
29. High-Performance Liquid Chromatography (HPLC): Detectors for HPLC
30. High-Performance Liquid Chromatography (HPLC): Quantitative Applications and Representative Method
31. High-Performance Liquid Chromatography (HPLC): Evaluation
32. Liquid�Solid Adsorption Chromatography
33. Ion-Exchange Chromatography
34. Size-Exclusion Chromatography
35. Supercritical Fluid Chromatography
36. Electrophoresis
37. Theory of Capillary Electrophoresis
38. Electrophoresis: Instrumentation
39. Capillary Electrophoresis Methods
40. Electrophoresis: Representative Method and Evaluation



Kinetic Methods of Analysis


1. Kinetic Methods of Analysis
2. Methods Based on Chemical Kinetics
3. Methods Based on Chemical Kinetics: Theory and Practice
4. Methods Based on Chemical Kinetics: Instrumentation
5. Methods Based on Chemical Kinetics: Quantitative Applications
6. Methods Based on Chemical Kinetics: Characterization Applications
7. Evaluation of Chemical Kinetic Methods
8. Radiochemical Methods of Analysis
9. Radiochemical Methods of Analysis: Theory and Practice
10. Radiochemical Methods of Analysis: Instrumentation
11. Radiochemical Methods of Analysis: Quantitative Applications
12. Radiochemical Methods of Analysis: Characterization Applications
13. Radiochemical Methods of Analysis: Evaluation
14. Flow Injection Analysis
15. Flow Injection Analysis: Theory and Practice
16. Flow Injection Analysis: Instrumentation
17. Flow Injection Analysis: Quantitative Applications
18. Flow Injection Analysis: Evaluation



Developing a Standard Method


1. Developing a Standard Method
2. Optimizing the Experimental Procedure
3. Optimizing the Experimental Procedure: Response Surfaces
4. Searching Algorithms for Response Surfaces
5. Mathematical Models of Response Surfaces
6. Verifying the Method
7. Validating the Method as a Standard Method
8. Two-Sample Collaborative Testing
9. Collaborative Testing and Analysis of Variance
10. What Is a Reasonable Result for a Collaborative Study?



Uality Assurance


1. Uality Assurance
2. Quality Control
3. Quality Assessment
4. Evaluating Quality Assurance Data: Prescriptive Approach
5. Evaluating Quality Assurance Data: Performance-Based Approach




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